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41.
为优化液相法一步制备磷酸铁锂(LiFePO4)技术,以七水合硫酸亚铁、磷酸二氢铵、一水合氢氧化锂为原料,通过添加十二烷基苯磺酸钠(SDBS)作为表面活性剂,采用液相水热法合成技术,一步合成了LiFePO4正极材料。研究了水热法一步合成技术对LiFePO4材料的组成、结构、形貌、粒度等的影响,通过电感耦合等离子体发射光谱仪(ICP-OES)、X射线衍射仪(XRD)、扫描电镜(SEM)、粒度分析仪等对材料进行了表征分析,并测试了材料的电化学性能。研究结果表明,合成得到的LiFePO4材料为微米级球形颗粒形貌的正交晶系非化学计量比的Li1.02Fe0.994PO4材料。电化学性能测试结果表明,在0.1C倍率下首次充、放电比容量分别为162.0、159.9 mA·h/g,库伦效率达到98.7%、倍率性能(以1C/0.1C保持率计)为92.3%,0.1C倍率循环100次容量保持率为96.4%,展现出良好的电化学性能。 相似文献
42.
Coupled large eddy simulation and the discrete element method are applied to study turbulent particle–laden flows, including particle dispersion and agglomeration, in a channel. The particle–particle interaction model is based on the Hertz–Mindlin approach with Johnson–Kendall–Roberts cohesion to allow the simulation of van der Waals forces in a dry air flow. The influence of different particle surface energies, and the impact of fluid turbulence, on agglomeration behaviour are investigated. The agglomeration rate is found to be strongly influenced by the particle surface energy, with a positive relationship observed between the two. Particle agglomeration is found to be enhanced in two separate regions within the channel. First, in the near-wall region due to the high particle concentration there driven by turbophoresis, and secondly in the buffer region where the high turbulence intensity enhances particle–particle interactions. 相似文献
43.
《Journal of the European Ceramic Society》2020,40(13):4655-4663
As a figure-of-merit, the rising ratio of crack propagation resistance to fracture initiation resistance indicates a reduction of the brittleness and enhances the thermal shock resistance of ordinary refractory ceramics. The significant nonlinear fracture behaviour is related to the development of a fracture process zone (FPZ). The universal dimensionless load–displacement diagram method is applied as a promising graphical method for the determination of R-curves for magnesia refractories showing different brittleness. By applying digital image correlation (DIC) together with the graphical method, the problems arisen with accurate determination of the fracture initiation resistance and the crack length are overcome. Meanwhile, the R-curve is subdivided with respect to the fracture processes, viz the fracture initiation, the development of FPZ and the onset of traction free macro-crack. With the simultaneous crack lengths evaluated from DIC, the contribution of each fracture process to the crack propagation resistance at certain loading stage is quantitatively presented. 相似文献
44.
为了成功预测竹林山煤矿综放高瓦斯矿井大采高工作面煤层瓦斯涌出量,以主采3号煤层为主要研究对象,针对3号煤层以往开采情况,通过布设测点测量其煤层瓦斯含量和了解相邻矿井瓦斯含量,采用分源预测法、回归法及统计法等预测方法得到了3号煤层瓦斯含量的分布规律,并绘制了3号煤层的瓦斯含量等值线图。对矿井不同生产时期的瓦斯含量进行预测,得到了生产前期、中期及后期采区的最大绝对瓦斯涌出量和最大相对瓦斯涌出量,说明了竹林山煤矿各个时期均属于高瓦斯矿井。 相似文献
45.
46.
本文基于横向积分离散纵标方程,解析得到横向积分通量中出射通量与入射通量的关系,并根据类似于扩散方程节块展开法的输运节块中子平衡方程形式,得到了一种高效的节块离散纵标法数值迭代策略。数值结果表明,本文提出的方法可行且数值结果正确。此外,粗网有限差分(CMFD)加速技术在节块离散纵标法中也取得了非常好的应用效果。 相似文献
47.
48.
《Ceramics International》2020,46(7):9025-9029
A series of phosphate glasses composed of (65-x)P2O5–15BaO–5Al2O3–5ZnO–10Na2O-xB2O3 (x = 0, 2, 4, 6, and 8 mol%) were successfully prepared using the melt-quenching method. The effects of the addition of boron trioxide (B2O3) on the physical, structural, and mechanical properties of the glasses were investigated. As the added content of B2O3 increased from 0 to 6 mol%, the glass exhibited increased density and transition temperature, and decreased molar volume, indicating optimization of the glass stability. Raman spectroscopy revealed that the introduction of B2O3 transformed the glass from a chain structure to a three-dimensional network structure, which enhanced the chemical stability of the glass by the cross-linking of long phosphate chains with boron ions. Regarding the mechanical properties, when the boron content was 6 mol%, the flexural strength of the glass was 41% higher than that of the undoped boron, while the Vickers hardness and Knoop hardness values increased by 20.58% and 7.05%, respectively, and the fracture toughness was slightly decreased. In general, improving the mechanical properties of phosphate glass is of great significance for increasing the applications of this glass. 相似文献
49.
对射频电缆幅相稳定性进行了介绍,阐述了射频测试电缆相位和幅度变化的因素,并详细分析了射频电缆相位性能以及幅度性能的不同测试方法,最后通过实测数据的展示,总结说明了在日常测试中该如何正确使用测试电缆。 相似文献
50.
Mohammed Heyouni Farid Saberi-Movahed Azita Tajaddini 《Computers & Mathematics with Applications》2019,77(1):77-92
In the first part of this paper, we investigate the use of Hessenberg-based methods for solving the Sylvester matrix equation . To achieve this goal, the Sylvester form of the global generalized Hessenberg process is presented. Using this process, different methods based on a Petrov–Galerkin or on a minimal norm condition are derived. In the second part, we focus on the SGl-CMRH method which is based on the Sylvester form of the Hessenberg process with pivoting strategy combined with a minimal norm condition. In order to accelerate the SGl-CMRH method, a preconditioned framework of this method is also considered. It includes both fixed and flexible variants of the SGl-CMRH method. Moreover, the connection between the flexible preconditioned SGl-CMRH method and the fixed one is studied and some upper bounds for the residual norm are obtained. In particular, application of the obtained theoretical results is investigated for the special case of solving linear systems of equations with several right-hand sides. Finally, some numerical experiments are given in order to evaluate the effectiveness of the proposed methods. 相似文献